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The crystal structures of several sterically overcrowded, non-​planar trialkylamines were determined. Some of these compounds are liquids at room temperature and suitable crystals were successfully grown on the diffractometer using the temperature gradient of the cold nitrogen beam.

by Michael Dieter Wörle
In-situ crystallization
Crystals were grown using temperature gradient of the cold nitrogen beam on the diffractometer.

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We got the external pagecover feature on an article for which we determined the crystal structures of several sterically overcrowded, non-​planar trialkylamines. Some of these compounds are liquids at room temperature and suitable crystals were successfully grown in-situ on the diffractometer using the temperature gradient of the cold nitrogen beam. (external pageChem. Eur. J. 11/2021).

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